Medicinal Plant

2015, v.6(Z4) 15-16+20

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Chemical Components in FRUCTUS GARDENIAE
Chemical Components in FRUCTUS GARDENIAE

Tao HUANG;Shuzhen MU;Xiaojiang HAO;Jianxin ZHANG;

摘要(Abstract):

[Objective]To research the chemical components in FRUCTUS GARDENIAE. [Methods]Silica column chromatography over silica gel,RP-18 reverse phase silica gel and Sephadex LH-20,as well as recrystallization were adopted. Structures of compounds were identified by1H-NMR,13C-NMR,ESI-MS,EI-MS and comparison with the data of literatures. [Results]A total of seven chemical compounds were isolated and purified from the ethanol extracts of FRUCTUS GARDENIAE,which were geniposide( 1),6α-hydroxygeniposide( 2),genipingentiobioside( 3),adian-5-en-3α-ol( 4),( 23Ζ)-cycloart-23-en-3β,25-diol( 5),7α-hydroxy sitosterol( 6) and 5,8-epidioxystigmasta-6,22-dien-3-ol( 7). [Conclusions] Compounds 4,5,6 and 7 were isolated from FRUCTUS GARDENIAE for the first time.

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基金项目(Foundation): Supported by the 2011 West Light Foundation of the Chinese Academy of Sciences

作者(Author): Tao HUANG;Shuzhen MU;Xiaojiang HAO;Jianxin ZHANG;

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